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Joseph I. Goldstein, Dale E. Newbury [et al.]. Scanning Electron Microscopy and X-Ray Microanalysis. (2017). (ISBN 978-1-4939-6674-5). (ISBN 978-1-4939-6676-9). (DOI 10.1007978-1-4939-6676-9).pdf
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2.2 · Critical Properties of Backscattered Electrons

.Figure 2.7 shows the results of similar Monte Carlo simulations for various elements as a function of surface inclination. As the surface tilt increases, η increases for all elements, converging toward unity at high tilt and grazing incidence for the incident beam.

SEM Image Contrast: “BSE Topographic Contrast—Number Effects”

This regular behavior of η vs. θ provides the basis for a contrast mechanism by which differences in the relative numbers of backscattered electrons depend on differences in the local surface inclination, which reveals the surface

21

 

2

 

 

 

topography. .Figure 2.8a shows an example of a pure material (polycrystalline silver) with grain faces inclined at various angles. The higher the inclination of the local surface to the incident beam, the higher will be the BSE signal, so that highly inclined surfaces appear bright, while dark surfaces are those nearly perpendicular to the beam. This image was prepared with a backscattered electron detector (discussed in the Electron Optics—Detectors module), which has a very large solid angle, so that backscattered electrons are collected with high efficiency regardless of the direction that they travel after leaving the specimen.

. Fig. 2.7  Monte Carlo calculations of electron backscattering from various tilted pure element bulk targets

Electron backscattering vs tilt angle

 

1.0

 

 

 

 

 

 

 

C

 

 

 

0.8

 

Al

 

 

 

 

Cu

 

 

 

 

 

 

 

coefficient

 

 

Ag

 

 

0.6

 

Au

 

 

 

 

 

 

 

 

 

 

 

Backscatter

0.4

 

 

 

 

 

 

 

 

 

 

0.2

 

 

 

 

 

0.0

 

 

 

 

 

0

20

40

60

80

Tilt angle (degrees)

a

b

5 µm

5 µm

. Fig. 2.8a SEM backscattered electron image of a topographically irregular surface of pure silver prepared with a large collection angle BSE detector. b SEM backscattered electron image of the same area,

prepared with a small collection angle BSE detector placed at the top of the image looking down